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How do I size a vertical mixer for wide batch ranges in order to scale from pilot to production?

Sizing a vertical mixer for wide batch ranges (typically a ratio of 1:5 to 1:10 between minimum and maximum fill) requires a combined consideration of geometry, drive power, bulk solids mechanics and process engineering characteristics. Purely geometric enlargement from pilot to production scale is not sufficient for this, since mixing kinetics and power input do not scale linearly.

First the batch spectrum and the usable volume are defined, and the fill level range is established. In practice, vertical mixers with a conical vessel and a screw or helical mixing tool can cover fill levels from approximately 20 % to 100 % of the usable volume.

The design must be laid out so that the mixing effect is reliably assured at minimum fill. Scale-up criteria must be derived from the pilot scale. The process variables are transferred from the pilot trials in order to make the mixing behaviour reproducible at production scale.

  • Geometric similarity: the ratio of vessel height to diameter (H/D) as well as the pitch angle and the diameter of the helix should remain as constant as possible, in order to retain comparable flow and conveying conditions.
  • Circumferential speed (v_tip): this is decisive for the shear energy input and thus for particle breakage and the break-up of agglomerates. For shear-sensitive products it is kept as similar as possible across the scales.
  • Specific power input (P/V): the power per volume is a characteristic value for dispersively dominated mixing processes.
  • Specific mixing intensity (P/m): the power per mass is a characteristic value for mixing intensity. At large volumes, a slightly reduced specific power input is often aimed at in favour of energy efficiency.
  • Mixing time characteristic (n·t_M): it is the product of rotational speed and mixing time. Where the geometry is similar, keeping this characteristic constant can be a robust guide value.

Geometric design for wide batch ranges

  • The vessel geometry has an H/D ratio that typically lies in the range of 1.2 to 1.8, in order to achieve good axial circulation.
  • A conical lower section with a cone angle of approximately 15–33° is customary.
  • In the tool design it must be taken into account that the screw/helix reaches down to the lowest point of the outlet, in order to avoid dead zones at a low fill level.
  • The gap between helix and wall should amount to only a few millimetres, in order to minimise wall build-up and dead zones without creating a risk of particles jamming.
  • The pitch ratio of the helix amounts to approximately 20 to 30 % of the helix diameter, in order to achieve a balanced relationship between axial conveying and radial circulation.
  • Flexibility for wide ranges: at extreme batch ratios, multi-stage mixing elements, adjustable tool heights or modular inserts can help to adapt the mixing zones to different fill heights.

Drive design and bulk solids mechanics

  • The hydrostatic pressure at the bottom grows with the fill height, so that the breakaway torque at full fill lies markedly above the steady-state operating torque.
  • In order to ensure reliable start-up under full load, a frequency-converter-controlled drive with a high starting torque (typically 2.0 to 2.5 times the rated torque) is to be preferred.

Mixing time and mixing quality across the fill range

Mixing time behaviour:

  • At a larger scale the particle paths lengthen statistically, which tends to lead to longer mixing times.
  • To limit the mixing time, the axial and the radial conveying rate of the mixer are to be calculated and optimised via geometry and rotational speed.

Homogeneity validation: the mixing quality is assessed in customary practice via the coefficient of variation (CV).

  • At wide batch ranges, a sampling matrix is advisable that provides for samples at minimum and maximum fill as well as at defined positions (top, middle, bottom).
  • Sampling systems at production scale must be designed so that they deliver representative samples during withdrawal without segregation.

Discharge behaviour and residual quantities

  • Large fill volumes increase the compaction pressure in the powder, particularly with fine-grained or cohesive bulk materials. The outlet diameter and the geometry of the discharge aids (e.g. bottom flaps, segment gates) must therefore be dimensioned critically.
  • With very small batches the percentage residual quantities are markedly higher. The discharge behaviour at minimum fill must therefore be examined specifically and, where necessary, optimised by an adapted outlet geometry or by re-conveying mechanisms.

Intermediate scale and practical verification

A direct jump from, for example, 100 l pilot volume to 5,000 l production volume entails high risks. An intermediate scale (factor 5–10) makes it possible:

  • to identify non-linear effects such as segregation, separation of fine particles or unexpected heat removal problems,
  • to check the drive design under real torque conditions at minimum and maximum fill,
  • to verify the discharge behaviour and the residual quantities across the entire batch range,
  • to establish the sampling matrix and the release criteria before investing in the production scale.

How amixon® secures the scale-up from the pilot plant into production

The mixing principle is identical across all scales. It does not matter which amixon® mixer is used: VM, HM, AM, KS, SH, AMK or Gyraton® – they all work on the same principle. All mixers display a high degree of congruence. This makes the formula universally applicable:

I_V = (π/4) · (D² − d²) · Φ · S · n · ζ

  • I_V: displacement or conveying volume flow
  • D/d: outer diameter/inner diameter of the helix
  • Φ: fill level (related to the usable volume)
  • S: pitch of the helix
  • n: rotational frequency (revolutions per second)
  • ζ: speed coefficient (tool-specific)

The core of the amixon® approach: trial and production mixers work with the same mixing system. The SinConvex® ribbon mixing tool conveys the mix upwards at the periphery and lets it flow downwards in the centre. This three-dimensional total flow has the same characteristic irrespective of the size. Scaling takes place via the restratification formula, that is via the conveying volume flow of the helical mixing tool and the restratification frequency derived from it – not via the rotational speed alone.

Mixing quality independent of fill level

amixon® mixers achieve the highest mixing qualities even at a low fill level (approximately 10 %), namely the technically ideal random mixture, which cannot be improved in practice. Batch sizes can vary within the same mixer without homogeneity having to be revalidated. This defuses the most critical moment in a scale-up: the first small production batches in the large machine.

A fine size range instead of jumps in scale

On request, amixon® manufactures mixer sizes in 100-litre increments from 100 to 50,000 litres (VM, HM, AM). The Gyraton® GM continues from 10 to approximately 100 m³ in 1 m³ increments. The step from the validated trial scale to the target size can be chosen as finely as desired, since there is no forced jump to the next catalogue size that would violate the similarity.

Validation before the investment

The amixon® pilot plant has 35 test units of various sizes available. Trials run with the original product, at real fill levels and within the planned temperature and pressure range. They are carried out, evaluated and documented together with amixon® experts. The parameters determined flow into the design of the production machine.

Manufacture in Paderborn as the quality foundation

amixon® develops and manufactures exclusively at the Paderborn works, with the greatest depth of fabrication and all components from Germany. As a certified welding company with European, Japanese, Korean and American qualifications, amixon® designs every apparatus as a one-off on the basis of the operator's URS. Quality control remains entirely in-house and every specification is verifiable down to component level. This manufacturing sovereignty also secures long-term supply. Every component can still be reproduced decades later.

Service across the entire life cycle

After commissioning, amixon® continues to stand at the operator's side: regular inspections and preventive maintenance secure availability, on request with predictive maintenance. Selected wear parts are supplied together with the initial delivery, and most spare parts are held at the Paderborn site as well as at the service bases in Japan and the USA. A lifetime spare parts service is thereby guaranteed, even where original suppliers cease to exist. Many amixon® machines have been in daily use for more than 30 years. Through modernisation and retrofitting they remain at the latest state of the art.